Microwave assisted batch and continuous flow synthesis of palladium supported on magnetic nickel nanocrystals and their evaluation as reusable catalyst
| Title | Microwave assisted batch and continuous flow synthesis of palladium supported on magnetic nickel nanocrystals and their evaluation as reusable catalyst |
| Publication Type | Journal Article |
| Year of Publication | 2017 |
| Authors | Nikam, AV, Kulkarni, AA, Prasad, BLV |
| Journal | Crystal Growth & Design |
| Volume | 17 |
| Issue | 10 |
| Pagination | 5163–5169 |
| Date Published | AUG |
| Type of Article | Article |
| ISSN | 1528-7483 |
| Abstract | Palladium nanocrystals (NCs) supported on nickel NCs (Pd/Ni) were synthesized in a continuous flow manner by the microwave-assisted method in the presence and absence of oleylamine. Parameters optimized for batch experiments were considered while performing continuous flow synthesis. The Pd/Ni NCs synthesized in the presence of oleylamine displayed good catalytic activity for hydrogenation of aromatic nitro compounds, and those bearing alkene, and alkyne moieties. The ferromagnetic character of the supporting nickel NCs allowed the recovery of the catalyst and these recovered catalysts could be reused several times. |
| DOI | 10.1021/acs.cgd.7b00639 |
| Type of Journal (Indian or Foreign) | Foreign |
| Impact Factor (IF) | 4.425 |
Divison category:
Chemical Engineering & Process Development
Physical and Materials Chemistry
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