Synthesis of nanocrystalline rutile

TitleSynthesis of nanocrystalline rutile
Publication TypeJournal Article
Year of Publication2005
AuthorsSamuel, V, Pasricha, R, Ravi, V
JournalCeramics International
Volume31
Issue4
Pagination555-557
Date PublishedJAN
Type of ArticleArticle
ISSN0272-8842
Keywordschemical preparation, Electron microscopy, powders, TiO2, X-ray methods
Abstract

Nanocrystalline titanium dioxide (TiO2) in the rutile phase has been obtained by homogeneous precipitation using urea and TiOCl2. A mixture of urea and TiOCl2 is heated on a hot water bath at 65-75 degrees C to precipitate rutile powders. X-ray diffraction (XRD) studies on these oven-dried powders indicated the formation of single-phase rutile. Raman scattering experiments were also performed to confirm the formation of the rutile phase. Transmission electron microscopy (TEM) investigations revealed the average particle size of these powders to be 40 nm. (c) 2004 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

Type of Journal (Indian or Foreign)

Foreign

Impact Factor (IF)2.758
Divison category: 
Catalysis and Inorganic Chemistry
Center for Material Characterization (CMC)
Physical and Materials Chemistry