Synthesis and MASNMR characterization of VPI-5 molecular sieve

TitleSynthesis and MASNMR characterization of VPI-5 molecular sieve
Publication TypeJournal Article
Year of Publication2007
AuthorsVenkatathri, N
JournalAsian Journal of Chemsitry
Volume19
Issue1
Pagination347-353
Date PublishedFEB
Type of ArticleArticle
ISSN0970-7077
Keywords3Q-MASNMR, FTIR, MASNMR, SEM, synthesis, TG/DTA, VPI-5, XRD
Abstract

The synthesized VPI-5 sample was characterized by XRD, SEM, FTIR, TG/DTA, Al-27, P-31 and 3Q MASNMR techniques, which shows that the sample was highly crystalline. Carbon and nitrogen analysis reveals that the sample contains no template molecules; however, TG/DTA analysis shows the presence of physisorbed template molecules. MASNMR results show the presence of two different types of aluminium and phosphorus, 3Q MASNMR shows the presence of two types of environmentally different tetrahedral aluminium, which are not observable by ordinary MASNMR along with known octahedral aluminium.

Type of Journal (Indian or Foreign)

Indian

Impact Factor (IF)

0.14

Divison category: 
Catalysis and Inorganic Chemistry