Nanosilica from Averrhoa bilimbi juice pre-treated rice husk: preparation and characterization

TitleNanosilica from Averrhoa bilimbi juice pre-treated rice husk: preparation and characterization
Publication TypeJournal Article
Year of Publication2023
AuthorsDominic, CDMidhun, Neenu, KV, Begum, PMSabura, Joseph, R, Rosa, Ddos Santos, Duan, Y, Balan, A, Ajithkumar, TG, Soumya, M, Shelke, A, Parameswaranpillai, J, Badawi, M
JournalJournal of Cleaner Production
Volume413
Pagination137476
Date PublishedAUG
Type of ArticleArticle
ISSN0959-6526
KeywordsAverrhoa bilimbi juice, Bioleaching, Nanosilica, rice husk
Abstract

The preparation of nanosilica from rice husk without using any concentrated mineral acids is a novel concept. This work proposes a bioleaching strategy to remove metallic impurities from rice husk for the preparation of nanosilica. Herein, nanosilica (BJRHS) was prepared by calcinating Averrhoa bilimbi juice pre-treated rice husks in a muffle furnace. The chemical and atomic structures of commercial precipitated silica (CS), rice husk ash (RHA), and BJRHS were analyzed using different analytical techniques. The optimal leaching time, calcination temperature, and calcination time were 1 h, 500 degrees C, and 6 h respectively. The particle size of BJRHS was found to be 6-12 nm, which is less than that of RHA and CS. The BET surface area of BJRHS (204 m2/g) was found to be greater than RHA (110.5 m2/g) and CS (172.1 m2/g). Mesoporous nanosilica with excellent surface area and purity was produced sustainably from rice husk which could be recommended to use in the field of catalysis, polymer technology, etc.

DOI10.1016/j.jclepro.2023.137476
Type of Journal (Indian or Foreign)

Foreign

Impact Factor (IF)

11.1

Divison category: 
Physical and Materials Chemistry
Database: 
Web of Science (WoS)

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