Microwave assisted convenient synthesis of quino[2,3-b][1,5]benzoxazepines
| Title | Microwave assisted convenient synthesis of quino[2,3-b][1,5]benzoxazepines |
| Publication Type | Journal Article |
| Year of Publication | 2009 |
| Authors | Sonar, SS, Sadaphal, SA, Pawar, SS, Shingate, BB, Shingare, MS |
| Journal | Chinese Chemical Letters |
| Volume | 20 |
| Issue | 5 |
| Pagination | 557-561 |
| Date Published | MAY |
| ISSN | 1001-8417 |
| Keywords | 3-b][1, 5]benzoxazepines, DBU/silica gel, Microwave irradiatiom, Quino[2, Solvent-free |
| Abstract | A convenient synthesis of quino[2,3-b][1,5]benzoxazepines from substituted 2-chloroquinoline-3-carbaldehyde and 2-hydroxyaniline by using stable, non-toxic and inexpensive catalyst 1,8-diazabicyclo-undecan-7-ene (DBU)/silica gel is described. This method affords the quino[2,3-b][1,5]benzoxazepines under the influence of microwave irradiation (360 W) in solvent-free conditions within short reaction times (2-3 min), giving high yields of products (93-96%). (C) 2009 Murlidhar S. Shingare. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved. |
| DOI | 10.1016/j.cclet.2009.01.031 |
| Type of Journal (Indian or Foreign) | Foreign |
| Impact Factor (IF) | 0.775 |
Divison category:
Organic Chemistry
Physical and Materials Chemistry