Low temperature route to prepare LaFeO3 and LaCoO3

TitleLow temperature route to prepare LaFeO3 and LaCoO3
Publication TypeJournal Article
Year of Publication2007
AuthorsJadhav, AD, Gaikwad, AB, Samuel, V, Ravi, V
JournalMaterials Letters
Volume61
Issue10
Pagination2030-2032
Date PublishedAPR
Type of ArticleArticle
ISSN0167-577X
KeywordsChemical synthesis, LaFeO3, Precipitation, transmission electron microscopy, X-ray diffraction
Abstract

A combination of digestion and further low temperature calcination to crystallize the product was employed to prepare LaFeO3 (LF) and LaCoO3 (LC) powders. Freshly co-precipitated lanthanum and ferric (or cobalt) hydroxide gels by sodium hydroxide were allowed to react at 100 degrees C under refluxing and stirring conditions for 4-6 h. These oven dried powders were heated at 450 degrees C to from crystalline LF (or LC) powders. The phase contents and lattice parameters were investigated by X-ray diffraction (XRD). Transmission electron microscope (TEM) investigations were carried out to examine the morphology and average particle size of these powders. (c) 2006 Elsevier B.V. All rights reserved.

DOI10.1016/j.matlet.2006.08.009
Type of Journal (Indian or Foreign)

Foreign

Impact Factor (IF)2.437
Divison category: 
Physical and Materials Chemistry