Low temperature route to prepare LaFeO3 and LaCoO3
Title | Low temperature route to prepare LaFeO3 and LaCoO3 |
Publication Type | Journal Article |
Year of Publication | 2007 |
Authors | Jadhav, AD, Gaikwad, AB, Samuel, V, Ravi, V |
Journal | Materials Letters |
Volume | 61 |
Issue | 10 |
Pagination | 2030-2032 |
Date Published | APR |
Type of Article | Article |
ISSN | 0167-577X |
Keywords | Chemical synthesis, LaFeO3, Precipitation, transmission electron microscopy, X-ray diffraction |
Abstract | A combination of digestion and further low temperature calcination to crystallize the product was employed to prepare LaFeO3 (LF) and LaCoO3 (LC) powders. Freshly co-precipitated lanthanum and ferric (or cobalt) hydroxide gels by sodium hydroxide were allowed to react at 100 degrees C under refluxing and stirring conditions for 4-6 h. These oven dried powders were heated at 450 degrees C to from crystalline LF (or LC) powders. The phase contents and lattice parameters were investigated by X-ray diffraction (XRD). Transmission electron microscope (TEM) investigations were carried out to examine the morphology and average particle size of these powders. (c) 2006 Elsevier B.V. All rights reserved. |
DOI | 10.1016/j.matlet.2006.08.009 |
Type of Journal (Indian or Foreign) | Foreign |
Impact Factor (IF) | 2.437 |