Efficient and convenient heterogeneous Cu/MCM-41 catalyst for the synthesis of 7,10,11,12-tetrahydrobenzo[c]acridin-8(9H)-one derivatives
| Title | Efficient and convenient heterogeneous Cu/MCM-41 catalyst for the synthesis of 7,10,11,12-tetrahydrobenzo[c]acridin-8(9H)-one derivatives |
| Publication Type | Journal Article |
| Year of Publication | 2023 |
| Authors | Dhengale, SD, Bhosale, TR, Shinde, SB, Rode, CV, Kolekar, GB, Anbhule, PV |
| Journal | Research on Chemical Intermediates |
| Volume | 49 |
| Pagination | 1581-1600 |
| Date Published | APR |
| Type of Article | Article |
| ISSN | 0922-6168 |
| Keywords | Benzo[c]acridine, dimedone, Heterogeneous Cu/MCM-41 catalyst, Multicomponent one-pot reaction |
| Abstract | An efficient and convenient method for synthesis of 7,10,11,12-tetrahydrobenzo[c]acridin-8(9H)-one derivatives using Cu/MCM-41 (20 mg) as heterogeneous catalyst. The advantages have an excellent product yield within a short time and easy work-up procedure, and the products have directly recrystallized from hot methanol with cost-effective catalyst. One-pot three-component reaction from aromatic aldehydes, cyclic 1,3-dicarbonyl compounds, and 1-naphthyl amine has been carried under ethanol as a solvent with reflux condition. Moreover, the catalyst can be recovered conveniently and reused efficiently, and recyclable. [GRAPHICS] . |
| DOI | 10.1007/s11164-023-04962-3 |
| Type of Journal (Indian or Foreign) | Foreign |
| Impact Factor (IF) | 3.134 |
Divison category:
Chemical Engineering & Process Development
Database:
Web of Science (WoS)