Effect of calcination cycles on the preparation of tin oxide based traditional drug: studies on its formation and characterization

TitleEffect of calcination cycles on the preparation of tin oxide based traditional drug: studies on its formation and characterization
Publication TypeJournal Article
Year of Publication2006
AuthorsWadekar, MP, Rode, CV, Bendale, YN, Patil, KR, Gaikwad, AB, Prabhune, A
JournalJournal of Pharmaceutical and Biomedical Analysis
Volume41
Issue4
Pagination1473-1478
Date PublishedJUN
Type of ArticleArticle
ISSN0731-7085
Keywordscalcination cycles, Oxidation, oxidation state of tin, Particle size, tin oxide, vanga bhasma
Abstract

The preparation method of metal based Indian traditional drugs involves conversion of a pure metal into its oxide by repeated high temperature calcination cycles. In this work, the effect of number of calcination cycles followed in the preparation of tin oxide based Ayurvedic drug, `vanga bhasma' was studied by a systematic characterization of the drug samples after various calcination stages. It was found that tin was in the form of Sn4+ state and that the formation of SnO2 proceeded step-wise through Sn(OH)(4). (c) 2006 Elsevier B.V. All rights reserved.

DOI10.1016/j.jpba.2006.03.032
Type of Journal (Indian or Foreign)

Foreign

Impact Factor (IF)3.169
Divison category: 
Biochemical Sciences
Catalysis and Inorganic Chemistry
Center for Material Characterization (CMC)