Coprecipitation technique to prepare Sr0.5Ba0.5Nb2O6

TitleCoprecipitation technique to prepare Sr0.5Ba0.5Nb2O6
Publication TypeJournal Article
Year of Publication2006
AuthorsA. Murugan, V, Gaikwad, AB, Samuel, V, Ravi, V
JournalBulletin of Materials Science
Volume29
Issue3
Pagination221-223
Date PublishedJUN
Type of ArticleArticle
ISSN0250-4707
KeywordsCeramics, Electron microscopy, ferroelectricity, Oxides, X-ray diffraction
Abstract

An aqueous mixture of ammonium oxalate and ammonium hydroxide was used to coprecipitate barium and strontium ions as oxalates and niobium ions as hydroxide under basic conditions. This precursor on calcining at 750 degrees C yielded Sr0.5Ba0.5Nb2O6 phase. This is a much lower temperature than that prepared by traditional solid state method (1000 degrees C) as reported for the formation of Sr0.5Ba0.5Nb2O6 (SBN). Transmission electron microscopic (TEM) investigations revealed that the average particle size was 80 nm for the calcined powders. The room temperature dielectric constant at I kHz was found to be 1100. The ferroelectric hysteresis loop parameters of these samples were also studied.

DOI10.1007/BF02706488
Type of Journal (Indian or Foreign)

Indian

Impact Factor (IF)0.895
Divison category: 
Center for Material Characterization (CMC)
Physical and Materials Chemistry