01326nas a2200229   4500008004100000022001400041245004000055210004000095260009900135300001200234490000700246520063900253653002500892653002400917653001200941653000900953653001800962100001400980700001600994700001201010856007401022       2005                        eng d  a0272-884200aSynthesis of nanocrystalline rutile0 aSynthesis of nanocrystalline rutile  aTHE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLANDbELSEVIER SCI LTDcJAN  a555-5570 v313 a<p>Nanocrystalline titanium dioxide (TiO2) in the rutile phase has been obtained by homogeneous precipitation using urea and TiOCl2. A mixture of urea and TiOCl2 is heated on a hot water bath at 65-75 degrees C to precipitate rutile powders. X-ray diffraction (XRD) studies on these oven-dried powders indicated the formation of single-phase rutile. Raman scattering experiments were also performed to confirm the formation of the rutile phase. Transmission electron microscopy (TEM) investigations revealed the average particle size of these powders to be 40 nm. (c) 2004 Elsevier Ltd and Techna Group S.r.l. All rights reserved.</p>10achemical preparation10aElectron microscopy10apowders10aTiO210aX-ray methods1 aSamuel, V1 aPasricha, R1 aRavi, V  uhttps://library.ncl.res.in/content/synthesis-nanocrystalline-rutile-0