01689nas a2200241   4500008004100000022001400041245010100055210006900156260009500225300001400320490000700334520080100341653002301142653001901165653001401184653002101198653000801219100001901227700002001246700003001266700001901296856013201315       2011                        eng d  a1533-488000aGlycerol mediated low temperature synthesis of nickel nanoparticles by solution reduction method0 aGlycerol mediated low temperature synthesis of nickel nanopartic  a25650 NORTH LEWIS WAY, STEVENSON RANCH, CA 91381-1439 USAbAMER SCIENTIFIC PUBLISHERScJUN  a5131-51360 v113 a<p>Phase pure Nickel nano-particles were synthesized by in-situ generation of nickel hydrazine hydrate complex (Ni-HH) followed by its decomposition in an alkaline glycerol medium. The synthesis can be performed in an open beaker with or without the use of surface protective reagents. By using the present method, Ni nano-particles can be prepared in large scale. The black nano-powders so-obtained were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED), Scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), Fourier transform infra-red (FTIR) spectroscopy and thermal analysis (TGA). XRD and SAED analysis revealed that the synthesized particles were pure crystalline nickel with FCC structure.</p>10aChemical Reduction10aNano-Particles10asynthesis10aTransition Metal10aXRD1 aSingh, Kalpana1 aKate, Kunal, H.1 aChilukuri, V., V. Satayan1 aKhanna, P., K.  uhttps://library.ncl.res.in/content/glycerol-mediated-low-temperature-synthesis-nickel-nanoparticles-solution-reduction-method-0