02223nas a2200253   4500008004100000022001400041245008300055210006900138260007300207300001200280490000800292520135900300653002501659653002301684653001801707653002001725653000801745100002001753700002001773700001901793700002401812700001901836856011401855       2006                        eng d  a0304-885300aMagnetic properties of NiCuZn ferrites synthesized by oxalate precursor method0 aMagnetic properties of NiCuZn ferrites synthesized by oxalate pr  aPO BOX 211, 1000 AE AMSTERDAM, NETHERLANDSbELSEVIER SCIENCE BVcOCT  a110-1190 v3053 a<p>Ni-Cu-Zn ferrites have been synthesized by employing co-precipitation technique using oxalate precursors. X-ray diffractograms did not show impurity phases, indicating single-phase formation of the ferrites. The diffractograms of oxalate complex decomposed at 650 degrees C show that ferritization is complete up to 650 degrees C. Lattice parameter a (angstrom) was found to decrease with the addition of Ni2+ which is attributed to ionic sizes of Ni2+ (0.69 angstrom), which replaces Cu2+ (0.72 angstrom). From the thermogravimetric studies it is observed that the experimentally observed total mass loss (%), agrees with theoretically calculated mass loss (%) indicating maintenance of requisite stoichiometry. Initial permeability (mu(i)) shows increase when Ni2+ is added up to x = 0.15 while for (x &gt; 0. 15), it decreases. The increase in initial permeability (mu(i)) is attributed to monotonic increase in Ms, and K-1 on addition of Ni2+. However, the microstructure and density (porosity) also influence mu(i) variations. The decrease in pi is attributable to increase of K-1. The composition with density 91.14% exhibits large mu(i) which also tends to increase with temperature up to 60 degrees C. Thus its usable range extends up to 60 degrees C. This samples has T-c near to 160 degrees C. (c) 2006 Elsevier B.V. All rights reserved.</p>10ainitial permeability10amagneticproperties10aMagnetization10aNiCuZn ferrites10aXRD1 aGhodake, S., A.1 aGhodake, U., R.1 aSawant, S., R.1 aSuryavanshi, S., S.1 aBakare, P., P.  uhttps://library.ncl.res.in/content/magnetic-properties-nicuzn-ferrites-synthesized-oxalate-precursor-method-001872nas a2200193   4500008004100000022001400041245009700055210006900152260008000221300001100301490000700312520113000319100002001449700002001469700002101489700001901510700002401529856012501553       2009                        eng d  a0964-172600aComplex permeability studies of Ni-Co-Zn ferrites synthesized by an oxalate precursor method0 aComplex permeability studies of NiCoZn ferrites synthesized by a  aDIRAC HOUSE, TEMPLE BACK, BRISTOL BS1 6BE, ENGLANDbIOP PUBLISHING LTDcDEC  a1250090 v183 a<p>Nanocrystalline Co-substituted Ni-Zn ferrites have been synthesized by employing a co-precipitation technique using oxalate precursors. The co-precipitated oxalates were decomposed in air at 650 degrees C for 1 h and the powder was sintered at 1000 degrees C. The phase formation of the sintered ferrite was confirmed by x-ray diffraction studies. The lattice parameter a (angstrom) increases with the addition of Co(2+) which is attributed to the large ionic size of Co(2+) (0.78 angstrom), which replaces Ni(2+) (0.74 angstrom). The crystallite size has been estimated by the Debye-Scherrer formula using the full width at half-maximum (FWHM) of the line broadening of the (311) reflection and it is found to be in the range of 25-28 nm. Also, with increasing cobalt content the magnetocrystalline anisotropy constant (K(1)) and magnetostriction constant (lambda(s)) increase, and the grain size decreases, hence the value of initial permeability mu(i) decreases. The saturation magnetization M(s) and magnetic moment (n(B)) do not show any significant variation for all compositions varying with the cobalt content.</p>1 aGhodake, J., S.1 aKambale, R., C.1 aKulkarni, S., D.1 aSawant, S., R.1 aSuryavanshi, S., S.  uhttps://library.ncl.res.in/content/complex-permeability-studies-ni-co-zn-ferrites-synthesized-oxalate-precursor-method-001866nas a2200217   4500008004100000022001400041245006500055210006400120260009900184300001400283490000700297520112100304653001301425653001701438653001101455653001201466100002501478700002401503700002201527856009901549       2009                        eng d  a0272-884200aNanostructured nickel ferrite: a liquid petroleum gas sensor0 aNanostructured nickel ferrite a liquid petroleum gas sensor  aTHE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLANDbELSEVIER SCI LTDcJUL  a1793-17970 v353 a<p>The present investigation deals with the synthesis of nanostructured nickel ferrite (NiFe(2)O(4)) and their liquid petroleum gas-sensing characteristics. The 15-20 nm size nickel ferrite has been synthesized at 700 degrees C by a simple molten-salt route using sodium chloride as grain growth inhibitor. These nanoparticles exhibit significantly high response towards liquid petroleum gas (LPG) in comparison with ethanol vapor, hydrogen sulfide, ammonia and hydrogen. The gas response towards various gases at their 200 ppm concentrations is investigated at 200-450 degrees C. Different characterization techniques have been employed, such as differential thermal analysis, X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and high resolution transmission electron microscopy (HRTEM) to study the crystallite size, structure and morphology. The results suggest possibility of utilization of the nanostructured nickel ferrite, without addition of any precious metal ion, as the LPG detector. (c) 2008 Elsevier Ltd and Techna Group S.r.l. All rights reserved.</p>10aFerrites10ananomaterial10aSensor10aSpinels1 aDarshane, Sonali, L.1 aSuryavanshi, S., S.1 aMulla, Imtiaz, S.  uhttps://library.ncl.res.in/content/nanostructured-nickel-ferrite-liquid-petroleum-gas-sensor-001856nas a2200229   4500008004100000022001400041245007900055210006900134260009900203300001400302490000700316520106100323653001501384653001401399653000901413653001501422100001801437700001801455700002201473700002401495856010701519       2012                        eng d  a0272-884200aInfluence of Pd-loading on gas sensing characteristics of SnO2 thick films0 aInfluence of Pdloading on gas sensing characteristics of SnO2 th  aTHE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLANDbELSEVIER SCI LTDcAUG  a4835-48440 v383 a<p>Nanocrystalline pristine and 0.5, 1.5 and 3.0 wt% Pd loaded SnO2 were synthesized by a facile co-precipitation route. These powders were screen-printed on alumina substrates to form thick films to investigate their gas sensing properties. The crystal structure and morphology of different samples were characterized by using X-ray diffraction, scanning electron microscopy and transmission electron microscopy techniques. The 3.0 wt% Pd:SnO2 showed response of 85% toward 100 ppm of LPG at operating temperature of 250 degrees C with fast response (8 s) and quick recovery time (24 s). The high response toward LPG on Pd loading can be attributed to lowering of crystallite size (9 nm) as well as the role of Pd particles in exhibiting spill-over mechanism on the SnO2 surface. Also selectivity of 3.0 wt% Pd:SnO2 toward LPG was confirmed by measuring its response to other reducing gases like acetone (CH3COCH3), ethanol (C2H5OH) and ammonia (NH3) at optimum operating temperature. (C) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.</p>10aLPG sensor10aPalladium10aSnO210aThick film1 aBagal, L., K.1 aPatil, J., Y.1 aMulla, Imtiaz, S.1 aSuryavanshi, S., S.  uhttps://library.ncl.res.in/content/influence-pd-loading-gas-sensing-characteristics-sno2-thick-films-002049nas a2200229   4500008004100000022001400041245009900055210006900154260009900223300001400322490000700336520120000343653002401543653001801567653002001585653000901605100001801614700001801632700002201650700002401672856012301696       2012                        eng d  a0272-884200aStudies on the resistive response of nickel and cerium doped SnO2 thick films to acetone vapor0 aStudies on the resistive response of nickel and cerium doped SnO  aTHE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLANDbELSEVIER SCI LTDcDEC  a6171-61790 v383 a<p>Undoped and Ni, Ce-doped nanocrystalline tin oxide were synthesized by co-precipitation route. Doped as well as undoped SnO2 compositions revealed single phase structure without any impurity. The lattice constant of SnO2 increases and the grain size decreases with doping of Ni and Ce. The responses of the sensing elements are evaluated by measuring the resistance change upon exposure to various test gases such as liquid petroleum gas (LPG), acetone, ethanol and ammonia. In comparison to LPG, ethanol, and ammonia the response towards acetone vapor increases markedly on simultaneous doping of Ni and Ce. For acetone vapors with 500 ppm at 300 degrees C, the undoped SnO2 shows 31% response, while with individual Ni or Ce doping it increases to 38 and 60%, respectively, however with simultaneous doping of Ni and Ce there is a significant enhancement up to 92%. The results of gas sensing measurements reveal that the thick films deposited on alumina substrates using screen printing technique give selectively a high response of (87%) with fast recovery (similar to 1 min) towards 100 ppm acetone at 300 degrees C. (c) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.</p>10a(Ni plus Ce)-doping10aAcetone vapor10aScreen-printing10aSnO21 aBagal, L., K.1 aPatil, J., Y.1 aMulla, Imtiaz, S.1 aSuryavanshi, S., S.  uhttps://library.ncl.res.in/content/studies-resistive-response-nickel-and-cerium-doped-sno2-thick-films-acetone-vapor-002109nas a2200241   4500008004100000022001400041245009800055210006900153260009500222300001100317490000700328520125300335653000801588653002001596653001101616653000901627100001801636700001801654700001801672700002201690700002401712856013101736       2013                        eng d  a1432-891700aAcetone vapour sensing characteristics of undoped and Zn, Ce doped SnO2 thick film gas sensor0 aAcetone vapour sensing characteristics of undoped and Zn Ce dope  aSTE 1C, JOSEPHS WELL, HANOVER WALK, LEEDS LS3 1AB, W YORKS, ENGLANDbMANEY PUBLISHINGcAPR  a98-1050 v173 a<p>The nanocrystalline materials of zinc and ceria doped tin oxide [(Zn+Ce)-SnO2] powders were synthesised by coprecipitation method and investigated for their sensing properties towards liquid petroleum gas (LPG), ethanol, ammonia and acetone vapour. The crystal structure and phase of the as synthesised and sintered powders were characterised by X-ray diffractometer and the microstructure by scanning electron microscopy. All the doped and undoped SnO2 compositions revealed single phase solid solution formation. Transmission electron microscope results indicated that well crystallised (Zn+Ce) doped SnO2 particles of size similar to 7 nm were obtained at the annealing temperature of 650 degrees C. The reduction in grain size of the metal oxide is a key factor to enhance the gas sensing properties. The doping of zinc, ceria in SnO2 has reduced the grain size and improved the gas response. The results of gas sensing measurements showed that the thick films deposited on alumina substrates using screen printing technique exhibited high response to acetone at an operating temperature of 300 degrees C. Further, the selectivity of the sensor towards acetone with respect to other reducing gases (LPG, ethanol and ammonia) was studied.</p>10aGas10aScreen printing10aSensor10aSnO21 aBagal, L., K.1 aPatil, J., Y.1 aBagal, K., N.1 aMulla, Imtiaz, S.1 aSuryavanshi, S., S.  uhttps://library.ncl.res.in/content/acetone-vapour-sensing-characteristics-undoped-and-zn-ce-doped-sno2-thick-film-gas-sensor-001797nas a2200253   4500008004100000022001400041245007900055210006900134260009900203300001400302490000700316520092500323653001201248653001501260653002301275653000801298100002201306700001901328700001801347700001901365700002201384700002401406856011301430       2013                        eng d  a0272-884200aLiquefied petroleum gas sensing performance of cerium doped copper ferrite0 aLiquefied petroleum gas sensing performance of cerium doped copp  aTHE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLANDbELSEVIER SCI LTDcJUL  a5901-59070 v393 a<p>Undoped and cerium (Ce) doped nanocrystalline copper ferrite (CuFe2O4) materials were synthesized via the molten-salt (M-S) method. Effects of Ce doping on the structural, morphological and gas sensing properties of the CuFe2O4 ferrite have been investigated. X-ray diffraction (XRD) analysis revealed the formation of spinel CuFe2O4. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) investigations showed that the synthesized ferrite is made up of very fine spherical nanoparticles. Moreover, the gas sensing properties of sintered samples were studied towards different reducing gases such as liquefied petroleum gas (LPG), acetone, ethanol and ammonia. The sample with 4% cerium doped CuFe2O4 (Ce4) showed the maximum gas sensitivity (86%) towards LPG with fast response time of 5 s and good recovery time of 68 s. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.</p>10aFerrite10aGas sensor10aMolten-salt method10aTEM1 aKhandekar, M., S.1 aTarwal, N., L.1 aPatil, J., Y.1 aShaikh, F., I.1 aMulla, Imtiaz, S.1 aSuryavanshi, S., S.  uhttps://library.ncl.res.in/content/liquefied-petroleum-gas-sensing-performance-cerium-doped-copper-ferrite-001867nas a2200241   4500008004100000022001400041245006200055210006200117260009900179300001200278490000700290520107800297653001201375653001201387653001501399653002301414653000801437100002201445700001901467700002201486700002401508856009301532       2014                        eng d  a0272-884200aNanocrystalline Ce doped CoFe2O4 as an acetone gas sensor0 aNanocrystalline Ce doped CoFe2O4 as an acetone gas sensor  aTHE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLANDbELSEVIER SCI LTDcJAN  a447-4520 v403 a<p>Nanocrystalline CoFe2-xCexO4 ferrites (x=0, 0.04, 0.08) were synthesized by using the inexpensive, simple and eco-friendly molten-salt (M-S) method. Effects of Ce doping on the structural, morphological and gas sensing properties of the CoFe2O4 ferrite were investigated. X-ray diffraction (XRD) analysis revealed the formation of spinel CoFe2O4. Transmission electron microscopy (TEM) investigations showed that the synthesized ferrite is made up of very fine spherical nanoparticles. Furthermore, the gas response of nanocrystalline ferrite materials was investigated in the temperature range of 200-450 degrees C toward the reducing gases like liquefied petroleum gas (LPG), acetone, ethanol and ammonia. The sensor response was found to be sensitive and selective toward acetone as compared to other reducing gases. It is observed that the addition of Ce (4 wt%) strongly influenced the response and the operating temperature of the sensor material and thus can serve as acetone-sensing sensors. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.</p>10aCoFe2O410aFerrite10aGas sensor10aMolten-salt method10aTEM1 aKhandekar, M., S.1 aTarwal, N., L.1 aMulla, Imtiaz, S.1 aSuryavanshi, S., S.  uhttps://library.ncl.res.in/content/nanocrystalline-ce-doped-cofe2o4-acetone-gas-sensor-001888nas a2200241   4500008004100000022001400041245008900055210006900144260006900213300001200282490000800294520105600302653002301358653001501381653001801396653001501414100001801429700001801447700002501465700002201490700002401512856011001536       2015                        eng d  a0925-400500aEffect of Pd and Ce on the enhancement of ethanol vapor response of SnO2 thick films0 aEffect of Pd and Ce on the enhancement of ethanol vapor response  aPO BOX 564, 1001 LAUSANNE, SWITZERLANDbELSEVIER SCIENCE SAcFEB  a383-3900 v2073 a<p>The undoped SnO2 and 4 wt% Ce-doped SnO2 were successfully synthesized by a facile co-precipitation route. The ternary systems were prepared by Pd-loading (0.5, 1.5 and 3.0 wt%) on the 4 wt% Ce-doped SnO2 nanoparticles. The structure and morphology of the nanocrystalline powders were investigated by X-ray diffraction, scanning electron microscopy and transmission electron microscopy techniques. The nanocrystalline powders were screen printed on the alumina substrates to form thick films to investigate their gas response properties. The gas response studies reveal that 4 wt% Ce-doped SnO2 with the loading of 3.0 wt% Pd exhibits high response (88%) towards ethanol (100 ppm) at an operating temperature of 250 degrees C with quick response (6 s) and rapid recovery (20 s). The high ethanol vapor response at lower operating temperature of this sensor is attributed to the spill-over mechanism of Pd particles present on the SnO2 surface and enhancement in alkalescence of SnO2 due to Ce-doping. (C) 2014 Elsevier B.V. All rights reserved.</p>10aCe-doped tin oxide10aGas sensor10aSemiconductor10aThick film1 aBagal, L., K.1 aPatil, J., Y.1 aVaishampayan, M., V.1 aMulla, Imtiaz, S.1 aSuryavanshi, S., S.  uhttps://library.ncl.res.in/content/effect-pd-and-ce-enhancement-ethanol-vapor-response-sno2-thick-films-001905nas a2200229   4500008004100000245012800041210006900169260000800238300001200246490000800258520111200266100001801378700001801396700001901414700001801433700001901451700001801470700001701488700002401505700001801529856012801547       2019                        eng d00aEnhanced energy density and stability of self-assembled cauliflower of Pd doped monoclinic WO3 nanostructure supercapacitor0 aEnhanced energy density and stability of selfassembled cauliflow  cMAR  a192-1990 v2253 aEnhanced electrochemical performance of WO3 nanostructures by engineering their morphology, structural and surface defect at nanoscale is feasible. Herein we report the effect of Pd doping on the morphological and electrochemical properties of WO3 at nanoscale prepared by a simple hydrothermal method. The synthesized pristine WO3 (cabbage like morphology) and Pd doped WO3 (cauliflower like morphology) are examined by using XRD, XPS, Raman spectra, BET, FE-SEM, TEM. The morphological investigation shows the effective rebuilding of nanosheets assembled cabbage shaped pristine WO3 into nanobricks assembled cauliflower shaped Pd doped WO3 with improvement in crystallinity, surface area and conductivity. As a result, the enhancement in the electrochemical performance of cauliflower shaped Pd-WO3 is recorded four times higher specific capacitance than pristine WO3. Additionally, the excellent cyclic stability (almost ten times higher than pristine WO3) up to 1100 cycles with nearly 86.95% capacity retention is observed in Pd-WO3 attributed to Pd content and highly modified structural arrangement.1 aGupta, S., P.1 aPatil, V., B.1 aTarwal, N., L.1 aBhame, S., D.1 aGosavi, S., W.1 aMulla, I., S.1 aLate, D., J.1 aSuryavanshi, S., S.1 aWalke, P., S.  uhttps://library.ncl.res.in/content/enhanced-energy-density-and-stability-self-assembled-cauliflower-pd-doped-monoclinic-wo3