01192nas a2200181 4500008004100000022001400041245010300055210006900158260011000227300001400337490000600351520042200357100001900779700002400798700002100822700003700843856013000880 2013 eng d a1759-966000aExpedient preparative isolation, quantification and characterization of limonoids from neem fruits0 aExpedient preparative isolation quantification and characterizat aTHOMAS GRAHAM HOUSE, SCIENCE PARK, MILTON RD, CAMBRIDGE CB4 0WF, CAMBS, ENGLANDbROYAL SOC CHEMISTRYcAUG a5386-53910 v53 a
Major basic limonoids from Neem fruits such as azadirone, epoxyazadiradione and azadiradione were isolated in preparative scale using an automated and rapid medium pressure liquid chromatography (MPLC)-based protocol. They were individually quantified using HPLC. An LC-ESI-MS/MS-based rapid identification technique was developed for the high-throughput screening of these limonoids in phytochemical extracts.
1 aHaldar, Saikat1 aPhapale, Prasad, B.1 aKolet, Swati, P.1 aThulasiram, Hirekodathakallu, V. uhttp://library.ncl.res.in/content/expedient-preparative-isolation-quantification-and-characterization-limonoids-neem-fruits-0